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A quantitative method for measuring the residual chloroform in neonatal serum was developed and applied to 23 clinical samples, which were collected from neonates exposed to chloroform in a stillbirth clinic. The chloroform remaining in the serum was reacted with imidazole on a magnesium chloride-coated column, followed by elution with 1:2-chloroform. The organic solvent was evaporated and then titrated with indigo carmine solution. The chloroform-imidazole complex formed in the serum was transferred to an aqueous solution by desorption with acetic acid, and finally determined by spectrophotometry. Chloroform was detected at a concentration of as low as 0.01 ppm in the serum. Normal values of the residual amounts in neonatal sera were 9.2 +/- 1.9 mg in infants less than 24 hours old, 7.9 +/- 2.6 mg in infants 24 to 48 hours old and 5.5 +/- 3.1 mg in infants older than 48 hours. This method offers a quick and reliable means of evaluation of the chloroform exposure during pregnancy.Q:
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